Journal
JOURNAL OF FLUORINE CHEMISTRY
Volume 128, Issue 1, Pages 34-39Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2006.09.013
Keywords
fluoroalkene; fluoroenone; ketone oxime ether; oxazaborolidine; enantioselective reductive amination
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From alpha-fluoroenones 2, a synthesis of (E) ketone oxime O-alkyl ethers 5 is reported with good to excellent yields. Then the first enantioselective reduction of these ketimines, via oxazaborolidine, is described with moderate to good enantiomeric excesses, leading to valuable chiral fluoroallylic amines 1. (c) 2006 Elsevier B.V. All rights reserved.
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