Journal
CHEMISTRY-A EUROPEAN JOURNAL
Volume 13, Issue 4, Pages 1032-1046Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.200601429
Keywords
fluorous-phase synthesis; heterocycles; organic synthesis; Pummerer reaction; samarium
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A fluorous, cyclative-capture strategy based on a new Pummerer cyclization process allows rapid access to tagged, heterocyclic frameworks. Convenient modification of the fluorous, heterocyclic scaffolds by using a variety of approaches including Pd-catalyzed cross-couplings is possible. Traceless, reductive cleavage of the fluorous-phase tag or oxidative cleavage and further elaboration, completes a strategy for the high-throughput, fluorous-phase synthesis of a diverse range of N-heterocycles.
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