Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 5, Issue 12, Pages 1970-1974Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b703646a
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Funding
- Engineering and Physical Sciences Research Council [EP/C508912/1] Funding Source: researchfish
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A calix[4] phyrin-(1,1,1,1) substituted with a 4-isothiocyanatophenyl group has been synthesised and used to attach the macrocycle to a solid support. The NCS group can also be used to further functionalise the calix[4] phyrin-(1,1,1,1) by reaction with amines and amino acids. Stability constants for anion binding by the calix[4] phyrin-(1,1,1,1) are reported and these show a clear ability to differentiate F- and HSO4- from Cl-, Br-, I- which can be detected by both NMR and UV-visible spectroscopy.
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