Journal
BULLETIN OF THE KOREAN CHEMICAL SOCIETY
Volume 33, Issue 6, Pages 1856-1860Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.5012/bkcs.2012.33.6.1856
Keywords
Nanocomposite; Sol-gel; SnO2/SiO2; Heterogeneous catalyst; 2-Arylbenzothiazoles
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SnO2/SiO2 nanocomposite has been synthesized by using sot-gel method. Prepared catalytic materials has been well characterized by using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), Fourier transform infrared spectroscopy (FT-IR), Brunauer-Emmer-Teller (BET) surface area, and temperature-programmed desorption of ammonia (NH3-TPD). SnO2/SiO2 nanocomposite catalyzed synthesis of 2-arylbenzothiazoles by the cyclocondensation of 2-aminothiophenol and aromatic aldehydes under reflux condition in 1:1 EtOH:H2O. After completion of the reaction, catalyst can be recovered efficiently and reused with consistent activity.
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