Journal
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN
Volume 82, Issue 7, Pages 891-895Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/bcsj.82.891
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- Ministry of Education, Culture, Sports, Science and Technology, Japan
- Research Association for Ishii Oxidation Technology
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One-pot Baeyer-Villiger oxidation of cycloalkanones was successfully achieved by allowing them to react with hydrogen peroxide generated in situ from benzhydrol and molecular oxygen assisted by N-hydroxyphthalimide (NHPI) and 2,2'-azobisisobutyronitrile (AIBN). This method provides an alternative synthetic route to lactones from cycloalkanones using sec-alcohols and molecular oxygen assisted by NHPI.
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