Journal
BULLETIN OF MATERIALS SCIENCE
Volume 34, Issue 7, Pages 1313-1317Publisher
INDIAN ACAD SCIENCES
DOI: 10.1007/s12034-011-0321-z
Keywords
alpha-Fe2O3; solvothermal; transmission electron microscope; X-ray diffraction
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Funding
- University Grants Commission (UGC), New Delhi
- Department of Science and Technology (DST), New Delhi
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Nanometer-sized alpha-Fe2O3 particles have been prepared by a simple solvothermal method using ferric acetylacetonate as a precursor. The products were characterized by X-ray diffraction (XRD), energy dispersive X-ray microanalysis (EDAX), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), transition electron microscopy (TEM), infrared spectroscopy (IR) and thermal analysis (TG-DTA). XRD indicates that the product is single-phase alpha-Fe2O3 with rhombohedral structure. Bundles of acicular shaped nanoparticles are seen in TEM images with an aspect ratio similar to 12; typically 8-12 nm wide and over 150 nm long. The alpha-Fe2O3 nanoparticles posses a high thermal stability, as observed on thermal analysis traces.
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