Journal
BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY
Volume 89, Issue 3, Pages 644-648Publisher
SPRINGER
DOI: 10.1007/s00128-012-0733-5
Keywords
Acetamiprid; Dissipation; Watermelon; Soil
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Residue dynamics of acetamiprid in watermelon and soil was studied in this paper utilizing liquid chromatography with tandem mass spectrometry (LC-MS/MS). The LODs for acetamiprid in whole watermelon, melon flesh and soil were 0.002 mg/kg. The fortified recoveries ranged from 73.7 % to 107.5 % with relative standard deviations (RSDs) of 1.7 %-5.9 %. Acetamiprid dissipated in watermelon and soil with the half-life 3.12-3.92 days and 1.18-1.46 days in two locations Beijing and Shandong provinces, respectively. In the terminal residue experiment, no higher residue than 0.01 mg/kg in melon flesh and 0.3 mg/kg in whole watermelon and soil were detected.
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