Journal
JOURNAL OF COORDINATION CHEMISTRY
Volume 68, Issue 14, Pages 2507-2519Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00958972.2015.1051974
Keywords
Imidazole dicarboxylate; Lead; Polymer; Crystal structure; Property
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Funding
- National Natural Science Foundation of China [21341002, J1210060]
- Program for New Century Excellent Talents in University [NCET-10-0139]
- Natural Science Foundation of Henan Education Department [13A150655]
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A 1-D coordination polymer, {[Pb(o-ClPhH2IDC)(2)]H2O}(n) (o-ClPhH3IDC=2-(2-chlorophenyl)-1H-imidazole-4,5-dicarboxylic acid) (1), a 2-D coordination polymer, [Pb-3(p-ClPhIDC)(2)(H2O)](n) (p-ClPhH3IDC=2-(4-chlorophenyl)-1H-imidazole-4,5-dicarboxylic acid) (2), and a 3-D polymer, [Pb(p-ClPhH2IDC)(2)](n) (3), have been obtained solvothermally and structurally characterized by elemental analyses, IR, and single-crystal X-ray diffraction. Although they were prepared with similar ligands and Pb2+, polymers 1-3 show distinct structures. The X-ray powder diffraction and thermal properties of the polymers have been investigated. The influence of the reaction conditions to the final products and coordination of the organic ligands are discussed.
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