Journal
COMPTES RENDUS CHIMIE
Volume 20, Issue 5, Pages 534-539Publisher
ELSEVIER FRANCE-EDITIONS SCIENTIFIQUES MEDICALES ELSEVIER
DOI: 10.1016/j.crci.2016.09.001
Keywords
Silver(I) complex; Single-crystal; Antibacterial effect; Tetrahedral; Bidentate
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Funding
- Payame Noor University
- Golestan University
- Czech Science Foundation [15-12653S, CZ.2.16/3.1.00/2451]
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We report the synthesis, characterization and crystal structure of a new mononuclear silver(I) complex, [Ag(catsc)(PPh3)(2)]NO3 (catsc = 3-phenylpropenalthiosemicarbazone). The complex was prepared by the reaction of catsc and AgNO3 in the presence of PPh3 and characterized by elemental analysis (CHN), FFIR, H-1, C-13 and P-31 NMR spectroscopy, and single-crystal X-ray diffraction. In the complex, catsc acts as a bidentate NS ligand while the nitrate is a counter ion. The silver ion is coordinated by a bidentate ligand and two PPh3 in the form of a distorted tetrahedron. In addition, the antibacterial effect of the complex was studied against the standard strains of two gram-positive (Staphylococcus aureus and Enterococcus faecalis) and two gram-negative (Escherichia coli and Pseudomonas aeruginosa) bacteria. (C) 2016 Academie des sciences. Published by Elsevier Masson SAS. All rights reserved.
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