Journal
BIOSCIENCE BIOTECHNOLOGY AND BIOCHEMISTRY
Volume 78, Issue 1, Pages 19-28Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/09168451.2014.877833
Keywords
lignan; kadangustin J; neolignan; 1,7-seco-2,7 '-cyclolignane
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Funding
- Marutomo Co.
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All the stereoisomers of butanol type 1,7-seco-2,7 '-cyclolignane were stereoselectively synthesized by employing (S)- and (R)-Evans' auxiliaries to construct the stereochemistry. (+)- and (-)-Kadangustin J and their diastereomers were also prepared. The optical purity of the synthesized butanol type 1,7-seco-2,7 '-cyclolignane was more than 99%ee.
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