Journal
BIORESOURCE TECHNOLOGY
Volume 101, Issue 4, Pages 1263-1267Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.biortech.2009.09.045
Keywords
D-Xylose; Superfine silica; Rice husk; Consecutive preparation
Funding
- China National Key Technology RD Programme [2008BAE66B00]
- Jilin Provincial Science & Technology Department governor fund [20075009]
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Rice husk is an abundant agricultural byproduct. In the present paper, research on consecutive preparation of D-xylose and superfine silica from rice husk is carried out. The optimum hydrolysis conditions of xylan in rice husk to D-Xylose are as follows: the concentration of H2SO4 is 4% (wt.%), the temperature is 130 degrees C, the ratio of rice husk mass (g) to H2SO4 Solution volume (ml) is 1:4 and the time is 2 h. The hydrolysis degree of xylan reaches 96.22% (wt.%). High purity (98.5%, Wt.%) D-Xylose is obtained from acid hydrolysis solution with the purification yield of 71.63% (wt.%). At the same time, the metal oxides in rice husk are efficiently dissolved by H2SO4. Residuals from H2SO4 pre-treatment are incinerated under 750 degrees C in stationary air for 15 min. Silica is obtained with the purity of 99.87% (wt.%). The superfine silica powder is obtained after ground and ultrasonic dispersion, with the diameter of 30-200 nm and specific surface 287.86 m(2)/g. (C) 2009 Elsevier Ltd. All rights reserved.
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