Journal
NEW JOURNAL OF CHEMISTRY
Volume 42, Issue 23, Pages 18894-18905Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8nj04443k
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Funding
- DBT, Government of India [BT/PR16958/NER/95/371/2015, BMB/2015/53]
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A synthetic strategy has been developed for pyrrolo[3,4-c]quinoline-1,3-diones. This synthetic protocol consists of sequential CeO2 catalyzed oxidative annulation followed by DDQ mediated dehydrogenation and N-demethylation. This sequential reaction strategy provides a wide range of fused tetrahydroisoquinolines and pyrrolo[3,4-c]quinoline-1,3-diones in good yields with excellent functional group tolerance. One of the synthesized pyrrolo[3,4-c]quinolines has been unambiguously established by its solid state structure using single crystal XRD. The photophysical properties of the synthesized pyrrolo[3,4-c]quinoline-1,3-diones were evaluated and some of them showed good fluorescence quantum yields.
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