Journal
POLYHEDRON
Volume 19, Issue 7, Pages 829-833Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0277-5387(00)00323-5
Keywords
antimonides; arsenides; metathesis; phosphides
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Nickel and cobalt pnictides have been synthesised using a liquid-mediated metathetical reaction of transition-metal dihalides with the appropriate sodium pnictide Na(3)E (E=P, As, Sb) in refluxing toluene for 48 h. Binary and ternary compounds have been prepared. Products were analysed by powder X-ray diffraction, scanning electron microscopy, energy dispersive analysis by X-rays, FT-IR, Raman and vibrating sample magnetometry. (C) 2000 Elsevier Science Ltd All rights reserved.
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