Journal
JOURNAL OF ORGANOMETALLIC CHEMISTRY
Volume 599, Issue 2, Pages 238-246Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/S0022-328X(00)00005-X
Keywords
bis(ferrocenyl)-1,3-diketones; chromium; tungsten; rhenium; iron; ruthenium; cobalt; palladium; C-C coupling; crystal structure
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The enolates of bis(ferrocenyl)-1.3-diketones are added to coordinated ethylene, cyclohexa- and cycloheptadienyl and heptatrienyl ligands of cationic complexes to give C-C coupling and formation of polynuclear compounds 1-10 and 13-15. Also palladium complexes of bis(ferrocenyl)-1,3-diketonates can function for these reactions. The structure of Fc-C(O)-CH[CH(2)CH(2)Fc(CO)(2)Cp]-C(O)-Fc was determined by X-ray diffraction. Threefold addition of [(eta(5)-C-6H7)Fe(CO)(3)](+) to the ligands of Co(acac)(3) was observed. (C) 2000 Elsevier Science S.A. All rights reserved.
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