Journal
HETEROCYCLES
Volume 53, Issue 5, Pages 1145-+Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.3987/COM-99-8792
Keywords
7-azaindole; 1-alkyl-7-azaindole; 1-alkyl-7-azaisatin; NVS-DMSO oxidation; reduced pressure condition
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1-alkyl-7-azaisatins are synthesized from the reaction of 1-alkyl-7-azaindoles with bromine in dichloromethane and subsequent oxidation with N-bromosuccinimide - dimethyl sulfoxide reagent. 1-Alkyl-7-azaindoles are readily available in high yields from the reaction of sodium salt of 7-azaindole with the appropriate alkyl halides in dimethylacetamide.
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