Journal
TETRAHEDRON LETTERS
Volume 41, Issue 24, Pages 4787-4790Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(00)00676-6
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Mitsunobu cyclization of o-[4-hydroxy-3-methyl-2(Z)-butenyl]pheno 2a effected selective seven-membered cyclization to give 3-methyl-2,5-dihydro-1-benoxepin la. Using this procedure, natural radulanin A and radulanin A methyl ether were synthesized effectively. (C) 2000 Elsevier Science Ltd. All rights reserved.
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