Journal
JOURNAL OF SOLID STATE CHEMISTRY
Volume 152, Issue 2, Pages 447-452Publisher
ACADEMIC PRESS INC
DOI: 10.1006/jssc.2000.8708
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The modification of the internal pore surface of mesoporous MCM-41 with 3-aminopropyl yielded amine group functionalized MCM-41, Copper(II) and manganese(II) phenanthroline complexes were grafted onto the functional MCM-41 via the coordination of the respective metal ion with the amine group, The metal ion complex functionalized mesoporous materials were characterized by powder X-ray diffraction (XRD), nitrogen adsorption/desorption at 77 K, solid state diffuse reflectance UV spectroscopy, and electron spin resonance (ESR) at 293 K as well as cyclic voltammetry. Preliminary studies suggested that the nature and electroactivity of metal ion complex functionalized MCM-41 differed significantly from those of metal ion complex impregnated MCM-41. (C) 2000 Academic Press.
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