Journal
ORGANIC LETTERS
Volume 2, Issue 14, Pages 2135-2138Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol006041h
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- NIGMS NIH HHS [GM-58833] Funding Source: Medline
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[GRAPHICS] Direct synthetic access to glycosyl-1-phosphates is accomplished with the dehydrative coupling of carbohydrate hemiacetals and dialkyl phosphates, employing dibenzothiophene-5-oxide and triflic anhydride. The procedure offers a new and versatile method for efficient preparation of a host of glycosyl-1-phosphates of variable structure with good control over anomeric selectivity.
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