Journal
TETRAHEDRON
Volume 56, Issue 30, Pages 5429-5434Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4020(00)00451-8
Keywords
fullerenes bisadduct; Diels-Alder reaction; o-quinodimethane
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The reaction of [60]fullerene with the o-quinodimethane species generated from 1,2-bis(bromomethyl)-4,5-dimethoxybenzene (1) was examined. Among possible regioisomers of bisadducts 2, seven isomers (trans-1, trans-2, trans-3, trans-4, e, cis-3, and cis-2) were isolated by HPLC and characterized on the basis of NMR, FAB-MS, and/or UV-Vis spectroscopies. (C) 2000 Elsevier Science Ltd. All rights reserved.
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