4.5 Article

Micropipes in silicon carbide crystals: Do all screw dislocations have open cores?

Journal

JOURNAL OF MATERIALS RESEARCH
Volume 15, Issue 8, Pages 1649-1652

Publisher

MATERIALS RESEARCH SOCIETY
DOI: 10.1557/JMR.2000.0236

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Micropipes in a 6H-SiC semiconductor wafer were studied by scanning electron and atomic force microscopy. The screw dislocations intersecting the wafer's surface were located by etch pitting, and their Burgers vectors determined by x-ray topography. The etch pits were eroded into smooth craters by ion beam etching to expose levels of dislocation Line from inside the sample's bulk. There a micropipe's diameter is distant from surface relaxation effects. Hollow cores (micropipes) were observed at the base of the craters whose screw dislocations had Burgers vectors of magnitude three multiples of the c-lattice parameter and higher. Screw dislocations with 1c and 2c Burgers vectors had no associated micropipes.

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