Journal
TETRAHEDRON
Volume 56, Issue 38, Pages 7423-7425Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4020(00)00654-2
Keywords
civetone; Ti-Claisen condensation; metathesis
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A highly efficient synthesis of civetone has been performed by joining two crucial reactions; (a) Ti-Claisen condensation and (b) intramolecular olefin metathesis using Grubbs' reagent. This synthesis includes not only a stepwise method (A) but also a one-pot method (B). (C) 2000 Elsevier Science Ltd. All rights reserved.
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