Journal
ORGANIC LETTERS
Volume 2, Issue 20, Pages 3047-3049Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol006111k
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[GRAPHICS] The title bipyridine ligand (+)-6(PINDY), prepared in five steps from (-)-beta-pinene, forms a stable complex with CuCl2 (8) that has been characterized by X-ray crystallography to reveal an unusual geometry at Cu. Triflate 9 proved to catalyze asymmetric allylic oxidation (10 --> 11; rt, similar to 30 min, 49-75% ee).
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