Journal
TETRAHEDRON LETTERS
Volume 41, Issue 43, Pages 8203-8206Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(00)01310-1
Keywords
6-bromopicoline; 6,6 '-dimethyl-2,2 '-bipyridine; electrosynthesis; reductive homocoupling; Ullmann coupling
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6-Bromopicoline can be reductively homocoupled to provide 6,6'-dimethyl-2,2'-bipyridine in high yield either by an Ni bpy catalysed electrosynthesis or by a catalytic modification of the Ullmann synthesis employing Pd(OAc)(2). Either procedure is operationally simple and represents a considerable improvement over most known syntheses of this important disubstituted bipyridine. (C) 2000 Elsevier Science Ltd. All rights reserved.
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