Journal
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
Volume 48, Issue 11, Pages 5211-5215Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jf000598u
Keywords
LC-MS/MS; lignin model compounds; lignols; arylglycerol-beta-aryl ethers; electrospray ionization mass spectrometry
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A LC-ES-MS/MS method for the identification of dilignols formed by the oxidative cross-coupling of coniferyl alcohol and apocynol has been developed. The identification is based on the generation of ammonium adduct ions [M + NH4](+) by electrospray ionization and thereafter the following fragmentation patterns for the selected precursor ions. Fragmentation of several arylglycerol-beta -aryl ether (beta -O-4) and phenyl coumarane (beta -5) model compounds were studied as a reference.
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