Journal
ORGANIC LETTERS
Volume 2, Issue 23, Pages 3535-3537Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0063205
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[GRAPHICS] Substituted 2-hydroxy-3-acetylfurans are synthesized by alkylation of tert-butyl acetoacetate with an alpha -haloketone followed by treatment of the obtained intermediate with trifluoroacetic acid (TFA). A second alkylation of the intermediate followed by treatment with trifluoroacetic acid provides access to disubstituted 2-methylfurans.
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