Journal
MICRON
Volume 31, Issue 6, Pages 659-667Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0968-4328(99)00076-1
Keywords
wool fibre; surface structure; lipid layer; atomic force microscopy; force-distance analysis; thin-film analysis
Categories
Ask authors/readers for more resources
Wool fibre surfaces have been treated by solvent cleaning which leaves the native covalently bound surface lipid layer intact, and by alcoholic alkali which removes the lipid layer. The resultant surfaces have been analysed by atomic force microscopy (AFM), with particular emphasis on force-distance (F-d) methods. Methodologies were developed for investigation in situ in water of both the surface topography and the characteristics of the lipid layer. Longitudinal surface texturing was resolved in images of wool fibre surfaces in air; the texturing remained prominent after exposure to water. High resolution F-d curves revealed features associated with the lipid layer. A simple formalism was used to show that the layer had a thickness of a few nm, and an effective stiffness of some 0.12 +/- 0.01 N/m. Strong adhesive interactions, equivalent to a pressure of 0.1 MPa, acted on the tip at the tip-to-substrate interface. The methodology and formalism are likely to be relevant in the broad field of thin-film analysis and for fibre technology. (C) 2000 Elsevier Science Ltd. All rights reserved.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available