Journal
TETRAHEDRON LETTERS
Volume 42, Issue 6, Pages 1127-1129Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(00)02168-7
Keywords
benzodiazepine; magnesium oxide; phosphorus oxychloride; ketones
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Magnesium oxide/phosphorus oxychloride (MOPO) was found to be an efficient reagent for the preparation of 1,5-benzodiazepine derivatives of o-phenylenediamine and ketones. This method is an easy, rapid, and high yielding reaction for the synthesis of 1,5-benzodiazepine derivatives. (C) 2001 Elsevier Science Ltd. All rights reserved.
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