Journal
CHEMICAL & PHARMACEUTICAL BULLETIN
Volume 49, Issue 3, Pages 324-326Publisher
PHARMACEUTICAL SOC JAPAN
DOI: 10.1248/cpb.49.324
Keywords
mediator; nitroxyl radical; electrocatalytic oxidation; N-alkyl-n-methylaniline; N-alkylformanilide
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Electrocatalytic oxidation of N-alkyl-N-methylanilines was studied using 4-benzoyloxy-2,2,6,6-tetramethylpiperidinyl- N-oxyl as a nitroxyl radical. The reaction with N-alkyl-N-methylanilines led to direct formation of N-alkylformanilides in the presence of H2O in reaction media in adequate conversion (>75.8%), high current efficiency (>89.2%) and high selectivity (>93.8%).
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