Journal
TETRAHEDRON
Volume 57, Issue 11, Pages 2179-2184Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4020(01)00049-7
Keywords
dimethyl acetylene dicarboxylate; thioamides; thiazoline
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A systematic study of the reactions of dimethyl acetylenedicarboxylate (DMAD) with heterocyclic thioamides has been carried out and a number of new 2-isoxazolyl-(8), imidazolyl-(13a,b and 17a), 1,2,3-triazolyl-(13d,e) and 1,2,3-thiadiazolyl (17b) thiazolines have been prepared. The higher reactivity of the thioamide group in comparison with the amino group in these reactions has been established. (C) 2001 Elsevier Science Ltd. All rights reserved.
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