Journal
CHEMISTRY OF MATERIALS
Volume 13, Issue 4, Pages 1413-1419Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cm001411h
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Sonochemical and microwave-assisted polyol reduction methods were used to prepare PbSe and PbTe. Products prepared by both methods were compared and analyzed by XRD, EDX, TEM, HR-TEM, elemental analysis, FT-IR, and thermal methods (DSC and TGA). In both methods almost pure lead chalcogenide phases were prepared, which were almost free of carbon (<0.08%,), but the morphology of the resultant nanoparticles was entirely different. The mechanism of formation for the lead chalcogenide nanoparticles for both microwave and sonochemical reactions is discussed.
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