Journal
JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS
Volume 44, Issue 5, Pages 365-372Publisher
JOHN WILEY & SONS LTD
DOI: 10.1002/jlcr.464
Keywords
C-13-labelled vitamin A analogs; C-13-retinyl acetate; 10,11,14,15-C-13(4)-retinyl acetate; 14,15-C-13(2)-retinyl acetate; retinoid synthesis; gas chromatography-combustion-isotope ratio mass spectrometry
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The synthesis of 10,11,14,15-C-13(4)- and 14,15-C-13(2)-retinyl acetate is described. The procedure uses a modified Wittig-Horner synthesis. By using the C-13 isotope, sensitive gas chromatography-combustion-isotope ratio mass spectrometry can be used for analysis in application to human isotope dilution studies.
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