Journal
THERMOCHIMICA ACTA
Volume 370, Issue 1-2, Pages 129-133Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/S0040-6031(00)00777-2
Keywords
nickel; copper; zinc; Schiff bases; thermogravimetry; differential scanning calorimetry
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The Schiff base complexes were prepared and characterised by UV, IR and NMR (H-1 and C-13) spectroscopy, elemental analysis and X-ray powder diffractometry. Free ligands and some new complexes were submitted to thermal analysis (TG and DSC) under dynamic air atmosphere. The differences in the decomposition profiles were related to the structure of isomers and decomposition intermediates were characterised according to their X-ray diffraction pattern. (C) 2001 Elsevier Science B.V. All rights reserved.
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