Journal
ORGANIC LETTERS
Volume 3, Issue 8, Pages 1193-1196Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0156547
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The [2 + 2] cycloaddition between [60]fullerene and benzyne generated from 4,5-dimethoxyanthranilic acid (4) afforded bisadducts 5 along with the monoadduct. All of the eight possible regioisomers were first isolated by HPLC and then characterized on the basis of MS, NMR, UV-vis, and CD spectroscopies.
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