Journal
MOLECULES
Volume 6, Issue 5, Pages 442-447Publisher
MDPI
DOI: 10.3390/60500442
Keywords
pinacol rearrangement; solid state reactions; AlCl3; Lewis acid
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A facile and efficient synthetic procedure for effecting the pinacol rearrangement catalyzed by AlCl3 in the absence of solvent is developed. The rearrangement product is obtained at room temperature in a few minutes and in almost quantitative yield. Benzylic pinacols rearrange under these conditions, while aliphatic pinacols do not react.
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