Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 66, Issue 12, Pages 4165-4169Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo0057250
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A microwave-enhanced, rapid and efficient homogeneous-phase version of the Sonogashira reaction is presented. It has been applied to the coupling of aryl iodides, bromides, triflates, and aryl chloride, as well as pyridine and thiophene derivatives with trimethylsilylacetylene. Excellent yields (80-95%) for substrates containing a large variety of substituents in different positions are obtained in 5-25 min.
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