Journal
TETRAHEDRON
Volume 57, Issue 26, Pages 5657-5662Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4020(01)00493-8
Keywords
Ambrox((R)); labdanolic acid; iododecarboxylation
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Iododecarboxylation of labdanolic acid (1), followed by dehydrohalogenation led to alkenes 4 and 12. Both compounds were converted into (1R,2R,4aS,8aS)-1-(2-hydroxyethyl)-2,5,5,8a-tetramethyldecahydro-2-naphthalenol (8), which was transformed via cyclization into (-)-Ambrox((R)) (9). (C) 2001 Elsevier Science Ltd. All rights reserved.
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