Journal
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY
Volume 56, Issue 6, Pages 831-838Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0584-8547(01)00173-2
Keywords
trace metal analysis; liquid analysis; laser breakdown spectroscopy
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This work reports on a simple, quick-freeze method for the quantitative analysis of trace metal ions in liquids applying the laser-induced breakdown spectroscopy (LIBS) technique. Using this procedure with calibrated samples, well-characterized linear working curves were determined for Na and Al water solutions over the 0.01-1% concentration range. This allowed detection limits of the order of ppm. In addition, optimum experimental conditions were found that allow the analysis to be carried out in a fast and very easy manner, without the limitations and difficulties found with liquid samples. The advantages of this simple and direct method, developed and patented by the Instituto Pluridisciplinar-UCM, are discussed, and potential applications for industrial analysis are also suggested. (C) 2001 Elsevier Science B.V. All rights reserved.
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