Journal
ORGANIC LETTERS
Volume 3, Issue 15, Pages 2387-2390Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol016202x
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[GRAPHICS] Exposure of cyclic acetals to 1-tert-butylperoxy-1,2-benziodoxol-3(1H)-one in the presence of tert-butyl hydroperoxide and potassium carbonate in benzene at room temperature results in oxidative ring cleavage to glycol monoesters via intermediate tert-butylperoxy ortho esters.
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