Journal
TETRAHEDRON-ASYMMETRY
Volume 12, Issue 13, Pages 1817-1823Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0957-4166(01)00323-8
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Disubstituted nitroalkenes were converted into enantiomerically enriched amines (isolated as their hydrochloride salts) with enantiomeric excesses of 88 to > 95% in three steps: (a) highly stereoselective conjugate addition of the potassium salt of 4-phenyloxazolidin-2-one; (b) radical-mediated removal of the nitro group: (c) cleavage of the oxazolidinone. (C) 2001 Elsevier Science Ltd. All rights reserved.
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