Journal
INORGANIC CHEMISTRY COMMUNICATIONS
Volume 4, Issue 8, Pages 381-383Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/S1387-7003(01)00199-X
Keywords
binuclear complexes; palladium; 2,2 '-biimdazole; X-ray structure
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Homobinuclear [(Pd(dppp))(2)(mu -biim)1(OTf)(2) (4) (dppp=bis(diphenylphosphino)propane. biim=2,2 \ -biimidazole, OTf = OSO2CF3) is accessible by the reaction of [Pd(dppp))(OTf)(2) (1) with H(2)biim (2) in the presence of an appropriate base. The structure of 4 was determined by X-ray crystallography. As a result thereof, the palladium atoms are located somewhat above and below the planar biim(2-) entity. (C) 2001 Elsevier Science B.V. All rights reserved.
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