Journal
JOURNAL OF MAGNETIC RESONANCE
Volume 151, Issue 2, Pages 153-227Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1006/jmre.2001.2336
Keywords
proton solid-state NMR; fast magic-angle spinning; multiple-quantum spectroscopy
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In the past few years, solid-state H-1 NMR spectroscopy under fast magic-angle spinning (MAS) has developed into a versatile tool for elucidating structure and dynamics. Dipolar multiple-quantum (MQ), in particular double-quantum (DQ), MAS spectroscopy has been applied to a variety of materials and provided unique insight, e.g., into the structure of hydrogen-bonded systems. This review intends to present solid-state H-1 DQ and MQ MAS spectroscopy in a systematic fashion with a particular emphasis on methodological aspects, followed by an overview of applications. (C) 2001 Academic Press.
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