Journal
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
Volume 9, Issue -, Pages 951-959Publisher
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.9.109
Keywords
3D printing; flow chemistry; flow IR; in-line analysis; imine reduction; imine synthesis; millifluidics; reactionware
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Funding
- Royal Society/Wolfson Foundation
- Leverhulme Trust
- University of Glasgow
- WestCHEM
- EPSRC
- EPSRC creativity@home scheme
- EPSRC [EP/I033459/1, EP/E062814/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/E062814/1, EP/I033459/1] Funding Source: researchfish
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We present a study in which the versatility of 3D-printing is combined with the processing advantages of flow chemistry for the synthesis of organic compounds. Robust and inexpensive 3D-printed reactionware devices are easily connected using standard fittings resulting in complex, custom-made flow systems, including multiple reactors in a series with in-line, real-time analysis using an ATR-IR flow cell. As a proof of concept, we utilized two types of organic reactions, imine syntheses and imine reductions, to show how different reactor configurations and substrates give different products.
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