Journal
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
Volume 7, Issue -, Pages 1124-1129Publisher
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.7.129
Keywords
azepinones; azides; continuous flow; nitrenes; photochemistry
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Funding
- Max Planck Society
- AstraZeneca RD
- Macclesfield, UK
- Fonds de Recherche sur la Nature et les Technologies, Quebec
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Photolysis of aryl azides to give nitrenes, and their subsequent rearrangement in the presence of water to give 3H-azepinones, is performed in continuous flow in a photoreactor constructed of fluorinated ethylene polymer (FEP) tubing. Fine tuning of the reaction conditions using the flow reactor allowed minimization of secondary photochemical reactions.
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