Journal
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
Volume 6, Issue -, Pages 784-788Publisher
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.6.83
Keywords
beta-cyclodextrin; calix[4]arene; click chemistry; poly(NIPAAM)
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We describe the calixarene-cyclodextrin-coupling via click reaction starting from 5,11,17,23-tetra-tert-butyl-25,27-dipropargylether- 26,28-hydroxy-calix[4] arene (calix[4]arene-dipropargylether) (2) onto 6I-azido-6I-deoxycyclomaltoheptaose (3) under microwave assisted conditions. The coupling was proven by MALDI-TOF mass spectrometry, H-1 NMR and IR-spectroscopy. The pH dependent supramolecular complex formation with poly(NIPAAM) bearing attached adamantyl units was investigated by dynamic light scattering (DLS) and turbidity measurements.
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