Journal
ORGANIC LETTERS
Volume 3, Issue 17, Pages 2729-2732Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol016333y
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- PHS HHS [R29-6M-55382] Funding Source: Medline
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[GRAPHICS] A simple, palladium-catalyzed method to convert aryl halides to the parent anilines using lithium bis(trimethylsilyl)amide (LiN(SiMe3)(2)) is reported. The reaction is catalyzed by Pd(dba)(2) and P(t-Bu)(3) and can be run with as little as 0.2 mol % of catalyst. The reaction is faster than competing generation of benzyne intermediates and, therefore, provides the aniline products regiospecifically.
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