Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 5, Issue 5, Pages 531-534Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op000109r
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A number of approaches to the synthesis of 2-chloro- and 2,6-dichloro-4-trifluoromethylpyridine are described. The first method for 2-chloro- and 2,6-dichloro-4-trifluoromethylpyridine is based on commercially available ethyl trifluoroacetate. An alternative access to 2,6-dichloro-4-trifluoromethyl pyridine uses trifluoroacetaldehyde as starting material. 2-Chloro-4-trifluoromethylpyridine is prepared from ethyl(trifluoroacetylvinyl)-ether in two steps.
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