Journal
ELECTROCHEMISTRY COMMUNICATIONS
Volume 3, Issue 9, Pages 483-488Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/S1388-2481(01)00158-8
Keywords
electrochemistry; IR spectroscopy; spectroelectrochemistry; TCNQ
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The efficiency and versatility of time-resolved FTIR spectroscopy has been used to follow concentration profiles of species produced during a cyclic voltammetric scan. It has been tested in situ and in resolved time, by probing the reduction of tetracyanoquinodimethane (TCNQ) on its first and second electrochemical wave. Besides the establishment of the method, the individual concentrations of TCNQ, of the monoanion and of the dianion were monitored at distinct infrared frequencies and the time derivatives of the concentration profiles were compared to the voltammograms. (C) 2001 Elsevier Science BN. All rights reserved.
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