Journal
JOURNAL OF HETEROCYCLIC CHEMISTRY
Volume 38, Issue 5, Pages 1227-1230Publisher
WILEY-BLACKWELL
DOI: 10.1002/jhet.5570380533
Keywords
-
Categories
Ask authors/readers for more resources
A novel synthesis of the title compound was achieved by direct amination using Vicarious Nucleophilic Substitution (VNS) methodology. Reaction of 1,1,1-trimethylhydrazinium iodide with 3,5-dinitropyrazole in DMSO produces 4-amino-3,5-dinitro-1H-pyrazole as a 1:1 crystal solvate with DMSO. Recrystallization from water yields the monohydrated crystal. Recrystallization of the monohydrate from butyl acetate yields the compound in pure form.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available