Journal
TETRAHEDRON LETTERS
Volume 42, Issue 36, Pages 6283-6286Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(01)01248-5
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An enantioconvergent synthesis of the aggregation pheromones (R)- and (S)-suleatol (6-methyl-5-hepten-2-ol) is described. Key steps in the deracemization strategy are sequential combinations of enzymatic resolutions and Mitsunobu inversions. Racemization-free Mitsunobu transformations have been carried out within 5 min by microwave irradiation, providing the desired sulcatyl acetates with clean inversion of chirality. (C) 2001 Elsevier Science Ltd. All rights reserved.
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