Journal
TETRAHEDRON
Volume 57, Issue 38, Pages 8167-8172Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4020(01)00786-4
Keywords
Baylis-Hillman chemistry; methyl 3-aryl-2-methylene-3-(prop-2-yn-1-yloxy)propanoates; chiral leaving group
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Asymmetric synthesis of (-)-methyl 3-aryl-2-methylene-3-(prop-2-yn-1-yloxy)propanoates in 25-40% enantiomeric purities via the reaction of methyl (2Z)-3-aryl-2-(bromomethyl)prop-2-enoates with prop-2-yn-1-ol in the presence of quinidine is described. (C) 2001 Elsevier Science Ltd. All rights reserved.
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